Methyl 3-nitrobenzoate [ 618-95-1 ]

Cas Number: 618-95-1
Product Code
117114
Product Name
Methyl 3-nitrobenzoate
Cas Number
618-95-1
Appearance
beige crystalline powder
Melting Point
78-80(lit.) ( ℃ )
Boiling Point
136.8 ( ℃ )
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mp  78-80 °C(lit.)
bp  279 °C(lit.)
Fp  279°C
Water Solubility  insoluble
BRN  392449
Stability: Stable. Incompatible with strong oxidizing agents.
CAS DataBase Reference 618-95-1(CAS DataBase Reference)
NIST Chemistry Reference 3-O2N-C6H4-COOCH3(618-95-1)
EPA Substance Registry System Benzoic acid, 3-nitro-, methyl ester(618-95-1)
Chemical properties: white needle crystal. Melting point ℃, boiling point ℃ 279 78. Slightly soluble in ethanol, ethyl ether, methanol, insoluble in water.
Use in organic synthesis.
USES as synthetic organic intermediates
Production method by benzoic acid methyl via nitrification. Will join dry sulfuric acid reaction pot, cold to 0-10 ℃, slowly add benzoic acid, methyl again drops add hair smoke of sulfuric acid and nitric acid mixture, the control system of temperature 5-15 ℃. Add finish, within 15 ℃ reaction 1h. Cooling, ice between nitro benzoic acid methyl exudates. Filtration, use alcohol washed oil strings, washing to finished products. Yield 80%.