Methyl 3-nitrobenzoate [ 618-95-1 ]
- Appearance
- beige crystalline powder
- Melting Point
- 78-80(lit.) ( ℃ )
- Boiling Point
- 136.8 ( ℃ )
mp | 78-80 °C(lit.) |
bp | 279 °C(lit.) |
Fp | 279°C |
Water Solubility | insoluble |
BRN | 392449 |
Stability: | Stable. Incompatible with strong oxidizing agents. |
CAS DataBase Reference | 618-95-1(CAS DataBase Reference) |
NIST Chemistry Reference | 3-O2N-C6H4-COOCH3(618-95-1) |
EPA Substance Registry System | Benzoic acid, 3-nitro-, methyl ester(618-95-1) |
Use in organic synthesis.
USES as synthetic organic intermediates
Production method by benzoic acid methyl via nitrification. Will join dry sulfuric acid reaction pot, cold to 0-10 ℃, slowly add benzoic acid, methyl again drops add hair smoke of sulfuric acid and nitric acid mixture, the control system of temperature 5-15 ℃. Add finish, within 15 ℃ reaction 1h. Cooling, ice between nitro benzoic acid methyl exudates. Filtration, use alcohol washed oil strings, washing to finished products. Yield 80%.